Tag Archives: manufacturing

Health Canada opens consultation on cleaning validation guidance

Health Canada has opened the consultation process to provide guidance on issues and topics related to the validation of equipment cleaning the removal of contaminants associated with previous products, residues of cleaning agents as well as control of potential microbial contaminants. This guidance is for pharmaceuticals biologicals and radiopharmaceutical product manufacturers. The purpose of this guidance is to ensure that such manufacturers remain compliant with good manufacturing practice (GMP).

more information can be found on the Health Canada website

EMA published guidance on specifications for herbal products

This new EMA guidance document provides general principles on the setting and justification of a uniform set of specifications herbal substances and preparations. Since a simplified registration procedure was established for traditional herbal medicinal products for human use the quality medicinal products is independent of its traditional use. More specifically the addition of vitamins to herbal products need to comply with all the relevant legislation guidance.

This document is concerned with the specific definitions as a list of tests, references to analytical and biological procedures and appropriate acceptance criteria a number of limit ranges and other criteria have been as described and established.

excerpt from regulations

full text here

This guidance document provides general principles on the setting and justification, to the extent possible, of a uniform set of specifications for herbal substances/preparations and herbal medicinal products to support applications for marketing authorisation or registration according to Directives 2001/82/EC and 2001/83/EC as amended. It should be read in conjunction with the ‘Guideline on quality of herbal medicinal products’ (EMA/CPMP/QWP/2819/00, EMA/CVMP/814/00, EMA/HMPC/201116/2005, as revised).
A simplified registration procedure was established for traditional herbal medicinal products for human use under Directive 2004/24/EC. The quality of a medicinal product is independent of its traditional use; therefore all general principles of quality also apply to traditional herbal medicinal products for human use. Traditional herbal medicinal products for human use may additionally contain vitamins or minerals. Concerning these products, this guideline describes specific aspects linked to mixtures of herbal substances/herbal preparations with vitamins and/or minerals. In addition, the quality, specifications and documentation for each vitamin and mineral have to comply with all relevant legislation and guidelines.

A specification is defined as a list of tests, references to analytical and biological procedures, and appropriate acceptance criteria, which are numerical limits, ranges, or other criteria for the tests described. It establishes the set of criteria to which a herbal substance/preparation or herbal medicinal product should conform to be considered acceptable for its intended use. “Conformance to specifications” means that the herbal substance/preparation or herbal medicinal product, when tested according to the listed analytical procedures, will meet the listed acceptance criteria. Specifications are legally binding quality standards that are proposed and justified by the manufacturer and approved by regulatory authorities.
Specifications are one part of a total control strategy for the herbal substance/preparation and herbal medicinal product designed to ensure product quality and consistency. Other parts of this strategy include thorough product characterisation during development, upon which specifications are based, adherence to the ‘Guideline on Good Agricultural and Collection Practice (GACP)’ (EMEA/HMPC/246816/2005) and Good Manufacturing Practice (GMP), and a validated manufacturing process, e.g., raw material testing, in-process testing, stability testing, etc.
In the case of herbal medicinal products, specifications are generally applied to the herbal substance, to the herbal preparation and to the herbal medicinal product. Specifications are primarily intended to define the quality of the herbal substance/preparation and herbal medicinal product rather than to establish full characterisation, and should focus on those characteristics found to be useful in ensuring the safety and efficacy of the herbal substance/preparation and herbal medicinal product.

EMA Announce Meeting on Lifecycles in Pharmaceutical Manufacturing

EMA Announce Meeting on Lifecycles in Pharmaceutical Manufacturing

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The Parenteral Drug Association, the International Society for Pharmaceutical Engineering, the Food and Drug Administration and the European Medicines Agency are creating a special joint conference dedicated to teaching the principles of International Conference on Harmonisation of Technical Requirements for Registration of Pharmaceuticals for Human Use (ICH) Q10. This is a unique opportunity to learn these principles from companies that have implemented a pharmaceutical quality system across the product lifecycle according to the ICH Q10 model.


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FDA Publish Guidance on Q11 Development and Manufacturing of Drug Substances

FDA Publish Guidance on Q11 Development and Manufacturing of Drug Substances

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This guideline describes approaches to developing process and drug substance understanding and also provides guidance on what information should be provided in CTD sections 3.2.S.2.2 – 3.2.S.2.6. It provides further clarification on the principles and concepts described in ICH guidelines on Pharmaceutical Development (Q8), Quality Risk Management (Q9) and Pharmaceutical Quality Systems (Q10) as they pertain to the development and manufacture of drug substance. A company can choose to follow different approaches in developing a drug substance. For the purpose of this guideline, the terms “traditional” and “enhanced” are used to differentiate two possible approaches. In a traditional approach, set points and operating ranges for process parameters are defined and the drug substance control  strategy is typically based on demonstration of process reproducibility and testing to meet established acceptance criteria. In an enhanced approach, risk management and more extensive scientific knowledge are used to select process parameters and unit operations that impact critical quality attributes (CQAs) for evaluation in further studies to establish any design space(s) and control strategies applicable over the lifecycle of the drug substance. As discussed in ICH Q8 for drug product, a greater understanding of the drug substance and its manufacturing process can create the basis for more flexible regulatory approaches. The degree of regulatory flexibility is generally predicated on the level of relevant scientific knowledge provided in the application for marketing authorisation. Traditional and enhanced approaches are not mutually exclusive. A company can use either a traditional approach or an enhanced approach to drug substance development, or a combination of both.



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Damien Bové is THE Drug Development and Regulatory Consultant (pharmaceutical or biotechnology), I work with my clients to define a drug development target, define a drug development strategy, define a regulatory strategy or define a commercial strategy. Our clients are generally raising funds or looking to license out their technology and we help them achieve it. If you want to know more don’t hesitate to get in touch.

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FDA Publishes Guidance on ANDAs and Impurities

FDA Publishes Guidance on ANDAs and Impurities

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This guidance provides recommendations on what chemistry, manufacturing, and controls (CMC) information sponsors should include regarding the reporting, identification, and qualification of impurities that are classified as degradation products in drug products when submitting:
• Original abbreviated new drug applications (ANDAs)
• ANDA supplements for changes that may affect the quantitative or qualitative degradation product profile
The guidance also provides recommendations for establishing acceptance criteria for degradation products (specifically, degradation products of the active ingredient or reaction products of the active ingredient with an excipient(s) and/or immediate container/closure system) in generic drug products. The guidance will replace an existing 1998 draft guidance of the same name.

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Damien Bové is THE Drug Development and Regulatory Consultant (pharmaceutical or biotechnology), I work with my clients to define a drug development target, define a drug development strategy, define a regulatory strategy or define a commercial strategy. Our clients are generally raising funds or looking to license out their technology and we help them achieve it. If you want to know more don’t hesitate to get in touch.

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Drug Regulators, EME (EMEA), Publish Concept Paper on Revision of the Guideline on Process Validation

Drug Regulators, EME (EMEA), Publish Concept Paper on Revision of the Guideline on Process Validation.

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This concept paper addresses the need to update the guideline on Process Validation. This guideline was originally adopted in February 2001. With the development of new ICH guidelines Q82, Q93 and Q104, this guideline is being reviewed in order to implement the concepts highlighted in the ICH guidelines.

The current guideline does not reflect the recent regulatory developments on Process Analytical Technology (PAT), Quality by Design (QbD) and Real-Time Release Testing (RTRT).

The current guideline was developed before the elaboration of the new ICH guidelines Q8 Pharmaceutical Development, Q9 Risk Management and Q10 Quality Systems. With these new guidelines, additional opportunities are available to verify the control of the process by alternative means to the manufacture of traditional process validation batches. The main objective of process validation remains that a process design yields a product meeting its pre-defined quality criteria. ICH Q8, Q9 and Q10 provide a structured way to define product critical quality attributes, design space, the manufacturing process and the control strategy. ICH Q8 refers to an ‘enhanced’ approach to pharmaceutical development which includes an alternative to the traditional process validation. Continuous process verification [see definition in ICH Q8(R2) glossary] can be utilised in process validation protocols for the initial commercial production and for manufacturing process changes for the continual improvement throughout the remainder of the product lifecycle. In contrast, the current note for guidance on process validation refers only to the more traditional approach of the manufacture of a number of validation batches to confirm that the process is under control. A revision to the note for guidance on process validation will bring it in line with ICH Q8, Q9 and Q10 documents and add the ‘enhanced’ approach to the current ‘traditional’ approach. The annexes of the current guideline will be included in the revised guideline. The revised guideline will also clarify to what extent ICH Q8, Q9 and Q10 should be followed when an applicant wishes to use alternative methods of process validation including continuous verification. The FDA guidance on process validation has been recently revised to take into account ICH Q8, Q9 and Q10. The revision to the note for guidance on process validation will provide a more harmonised approach.

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Damien Bové is THE Drug Development and Regulatory Consultant (pharmaceutical or biotechnology), I work with my clients to define a drug development target, define a drug development strategy, define a regulatory strategy or define a commercial strategy. Our clients are generally raising funds or looking to license out their technology and we help them achieve it. If you want to know more don’t hesitate to get in touch.

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ida consultants freestrategyconsultation 515x64 Drug Regulators, EME (EMEA), Publish Concept Paper on Revision of the Guideline on Process Validation

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Drug Regulators, FDA, Publish Draft Guidance on Manufactures of Human Cells,Tissues and Cellular and Tissue Based Products

Drug Regulators, FDA, Publish Draft Guidance on Manufactures of Human Cells,Tissues and Cellular and Tissue Based Products

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The FDA, are issuing this guidance to provide, establishments that manufacture human cells, tissues, and cellular and tissue-based products (HCT/Ps), with recommendations for complying with Current Good Tissue Practice (CGTP) requirements under Title 21 Code of Federal Regulations, part 1271, subpart D (21 CFR part 1271, subpart D), and requirements under 21 CFR part 1271, subpart E (Additional requirements for establishments described in
§ 1271.10). This guidance also addresses whether the establishment registration and HCT/P listing requirements under 21 CFR part 1271, subparts A and B apply in certain instances.

Damien Bové works as a drug development consultant (pharmaceutical or biotechnology) and regulatory consultant, we work with our clients to define a drug development target, define a drug development strategy, define a regulatory strategy or define a commercial strategy. Our clients are generally raising funds or looking to license out their technology and we help them achieve it. If you want to know more don’t hesitate to get in touch.

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This guideline ap
recombinant vaccines for the prevention and treatment of infectious disease, and provides guidance on quality, non-clinical and clinical aspects.
ida consultants freestrategyconsultation 515x64 Drug Regulators, FDA, Publish Draft Guidance on Manufactures of Human Cells,Tissues and Cellular and Tissue Based Products

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“Please note that the pages on this website are designed to provide you with general information only. We make no warranties, representations or undertakings about any of its content. This includes the completeness, accuracy and fitness for any particular purpose, or the content of any third party site referred to or accessed through it. You are personally responsible for ensuring that the information is correct and we will not be held liable or accountable for any mistakes that occur.”

Drug Regulators Publish, Guidance on Use of Accredited Persons Under the Accredited Persons Inspection Programme

Drug Regulators, FDA, Publish Guidance on Selection of Accredited Persons.

Manufacturer’s Notification of the Intent to Use an Accredited Person under the Accredited Persons Inspection Program Authorized by Section 228 of the Food and Drug Administration Amendments Act of 2007 (FDAAA).

Manufacturers Of Medical Devices May Be Eligible To Have Third-Party Inspections Of Their Establishments

On September 27, 2007, the Food and Drug Administration Amendments Act of 2007 (FDAAA) amended the voluntary third-party inspection program initially established by law in 2002, and applicable to manufacturers of class II or class III medical devices who meet certain eligibility criteria (see 21 USC §374(g)). The Inspection by Accredited Persons Program (AP Program), allowed eligible manufacturers to elect to have third parties that have been accredited by FDA (Accredited Person or AP) conduct some of their inspections instead of FDA. Under that 2002 law, manufacturers of eligible medical devices requested prior approval to use an AP instead of FDA staff to conduct a Quality Systems (QS) regulation inspection of their facilities.

If you would like more detail in this area please get in touch with Damien Bové damien.bove@idaconsultants.com

Damien Bové works as a drug development consultant (pharmaceutical or biotechnology) and regulatory consultant, we work with our clients to define a drug development target, define a drug development strategy, define a regulatory strategy or define a commercial strategy. Our clients are generally raising funds or looking to license out their technology and we help them achieve it. If you want to know more don’t hesitate to get in touch.

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ida consultants freestrategyconsultation 515x64 Drug Regulators Publish, Guidance on Use of Accredited Persons Under the Accredited Persons Inspection Programme

Eden Biodesign – Accelerating Novel Vaccine Development

  • I have just spent a good 30mins listening to a webinar from Eden Biodesign. The topic of discussion was the challenges facing those developing Novel Vaccines and what Eden are doing to help overcome them.

Challenges

  • Lots of vaccines are becoming “small molecule like”
  • There is no platform technology for novel vaccine production everything is bespoke
  • There is limited support available (regulatory and production expertise)

Dynamic Market

  • mAb is a large market – in vaccines its now bigger than small mollecules
  • Its a growing market
  • Deep product pipeline

Novel Vaccines

  • New Producs constantley emerging
  • Pandemic infection preparation
  • Growing markets in developing world
  • Bioterrorism preparation
  • Offer good economics
  • Growth of therapeutic vaccines
  • Still lots of interest from Big Pharma

Manufacturing changes

  • Traditional techniques are still important
  • Mammalian cell lines
  • Microbial fermentation
  • Chromatographic purification techniques

All associated with analytical challanges

Monoclonals are becoming “small molecule like”

  • Mainstream technology
  • Platform manufacturing is now becoming a reality
  • Greater availability of expertise
  • Commercial scale ready systems available
  • Easily outsources production
  • Regulations have matured, comparability guidelines and FDA, CDER control rather than CBER control

Challenges for novel vaccine process development

  • Speed, robustness and transferability
  • Cost of goods pressure
  • Production expertise is limited
  • Hard to characterise
  • Challenging to validate and reproduce processes
  • No pre-determined acceptance criteria
  • No dominant production platform
  • Constraints on process change
  • Processes can be difficult to scale up and transfer
  • Limited expert skills and knowledge available

In order to overcome these issues people are investing in dedicated facilities early on which significantly raises the financial risks associate with a programme.

How are Eden meeting these challenges

  • Innovative facility design
  • New analytical tools
  • More platform like technologies
  • knowledge management focused on product quality
  • Contained facilities
  • Disposable technologies
  • Skid mounted unit operations (facilities that can be flexible to requirements)
  • Wide range of expertise and experience in house

Important regulatory changes – FDA published a CFR that Live Vaccines can be be produced in multi product facilities.

This webinar series is ongoing so I suggest you have a look (link)

Damien Bové works as a drug development consultant (pharmaceutical or biotechnology), we work with our clients to define a development target, define a development strategy, define a regulatory strategy or define a commercial strategy. Our clients are generally raising funds or looking to license out their technology and we help them achieve it. If you want to know more don’t hesitate to get in touch using the contact form or email Damien at damien.bove@idaconsultants.com